Jpn. J. Appl. Phys. 5 (1966) pp. 886-899  |Next Article|  |Table of Contents|
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Theoretical Calculation of Fluorescent X-Ray Intensities in Fluorescent X-Ray Spectrochemical Analysis.

Toshio Shiraiwa and Nobukatsu Fujino

Physics Section, Central Research Laboratories, Sumitomo Metal Industries

(Received April 15, 1966)

The theoretical formulas of the fluorescent x-ray intensity (the primary, the secondary and the tertiary fluorescent x-rays) are obtained and actual calculations are made for nickel-iron, iron-chromium, and nickel-iron-chromium alloys. In the calculation, the continuous intensity distribution of the irradiating x-rays for the wavelength is taken into account. The theoretical results agree with the experiments very well, the deviations being 1% at most, and it is concluded that the theoretical estimation of the fluorescent x-ray intensity emitted from samples of various composition is possible. The matrix effect, absorption effect, and enhancement effect are evaluated from the present theory. In the enhancement effect, secondary fluorescent x-rays are quite significant (for instance, the chromium secondary fluorescent x-rays from Cr 2% and Fe 98% alloy reach the 55% of the chromium primary fluorescent x-rays and they can not be neglected), but the tertiary fluorescent x-rays are only a few per cent. The usual approximation methods, where the irradiating x-rays are assumed as monochromatic rays and the secondary fluorescent rays are not taken into consideration are also discussed and their meaning is made clear.

URL: http://jjap.ipap.jp/link?JJAP/5/886/
DOI: 10.1143/JJAP.5.886


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References | Citing Articles (113)

  1. K. Glocker and H. Schreiber: Ann. Phys. 85 (1928) 1087[Elsevier].
  2. E. Gillam and H. T. Heal: Brit. J. Appl. Phys. 3 (1952) 353.
  3. J. Sherman: Spectrochim. Acta 7 (1955) 283.
  4. H. T. Beattie and R. M. Brissey: Anal. Chem. 26 (1954) 980.
  5. A. H. Compton and S. A. Allison: X-ray in Theory and Experiment 2nd ed. (D. Van Nostrand Co., Ltd., New York 1935).
  6. The International Union of Crystallography: International Tables for Crystallography, Vol. III. (Kynoch Press, Birmingham 1962).

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